Central Research Instrumentation Facility(CRIF)

IIT Bhubaneswar

Central Research Instrumentation Facility

The CRF caters to the needs of researchers within the Institute as well as outside; both academic and industrial users enjoy the benefits of the sophisticated facilities housed here. Such a facility represents a key commitment for preserving and raising the efficiency of research to the international standards. While a number of tools are housed in our campus. We feel proud to offer these services to everyone through a complete online booking system with minimal human interventions.

Equipments

Field Emission Scanning Electron Microscopy (FESEM)

Make: ZEISS Model: MERLIN Compact

Gemini I column with crossover free beam path

Resolution: 0.8nm at 15 kV,1.6 nm at 30 kV

Large specimen chamber 330mm inner diameter and 270 mm height

Magnification Range: 12 – 2.000.000x

Accelerating voltage: 50 V to 30 kVe

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Nuclear Magnetic Resonance (NMR) Spectrometer

Make: Bruker

Bruker Avance III 400 is equipped with two probes which cover a wide range of experiments, with capabilities ranging from high sensitivity observation of proton, carbon, phosphorous, and fluorine to allowing observation of a large number of more exotic nuclei. 400 MHz, 2-channel spectrometer with Z-gradient and equipped for gradient shimming

Standard probe: 5mm BBFO Z-gradient SmartProbe with Automatic Tune and Match.

1H, direct- and indirect-detection (HSQC, HMBC, etc.) of heteronuclei.

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Single Crystal X-ray Diffractometer

Make: Bruker Model: D8 VENTURE

Dual Wavelength System with sealed tube Mo and High brightness Cu Sources.

X-ray Generator Out put power max 3000 W

High Voltage : 20- 60 kV

Current : 5- 80 mA

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Powder X-ray Diffractometer

Make: Bruker Model: D8 ADVANCE

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Liquid Chromatograph Mass Spectrometer

Make:Thermo Scientific Model: EXACTIVE PLUS Orbitrap-based benchtop MS system with high resolution, precise mass accuracy and high sensitivity.

Mass range: 50 to 6,000 Da

Resolution: 140,000 at m/z 200 at a scan repetition rate of 1.5 Hz.

Mass accuracy: < 3 ppm RMS error with external calibration (under specified conditions) for MS and MS/MS; < 1 ppm RMS error with internal calibration (under specified conditions) for MS and MS/MS

Sensitivity: sub ppb range for small molecules (pesticides and similar compounds)

Dynamic range: > 5,000 (in single spectrum)

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